The monomer (di alcohol) is not soluble in chloroform or dichloromethane, and the solubility of di-isocyanate is not an issue. I am using tin octonate as catalyst.
Can you provide detailed information about raw materials you are using? Please keep in mind that when choosing a solvent for polyurethane synthesis, you should ensure that both monomers (raw materials) and the formed PU are soluble in the reaction medium. Otherwise, the polymer will precipitate out of solution. The most suitable solvents for making PU include dipolar aprotic solvents such as DMF, DMAc, NMP, DMSO - the last one being preferred due to its low toxicity, high solvency and miscibility with water (the polymer can be collected by precipitation with water).
Please let us know the composition so that we could provide you with the optimal synthesis conditions of your PU system.
Hi Pawel, due to the patent protection issue, I can not disclose the actual structure, However, you provided me very good information regarding the synthesis. Thank you so much.