# 10 at% Zr was doped in barium titanate at titanium site.
# XRD confirms the proper phase formation.
# curie temperature should be around 60 degree C.
# Dielectric Constant is just decreasing with increasing temperature.
# the pattern of loss tan is okay (minimum near transition temperature).
What should be the problem with this?
The machine is working fine and this is happening for all the samples of this series.