Dear Peptide Chemists, in SPPS we forgot to deprotect the Fmoc protection group of the N-term on a complicated enough product. It's not cleaved from the resin with standard TFA protocol, washed with ether and redissolved in AcN/H2O. Do you have a stable protocol for Fmoc deprotection in liquid phase? We usually use 20% piperidine on the solid phase synthesizer.

Thanks so much!