rGO was obtained by reducing GO that was synthesized by modified hummers method. If it is possible to produce thin flakes of rGO from a bult rGO, how could we characterize so that I can prove the presence of thin flakes?
Hello Lokesh, Graphene oxide can be synthesized from graphite by a few methods, one of which is modified hummer's method. The graphene oxide itself is in the range of 1- 2 nm if it yields appropriately.
The need for reduction is to make the material conducting because the GO shows more resistance due to the functional groups (C–OH, C–O–C, C=O, and O=C–OH groups) attached to it
This reduction can be made either by chemical or thermal. The following links give an idea of them.
1. Chemical reduction: This method is accurate and can be produced the same conductivity multiple times. (More repeatable). But need chemicals to carry out and is difficult compared to thermal reduction.
2. Thermal reduction: This method is simple and doesn't need chemicals for reduction. But difficult to achieve repeatability (same conductivity every time)
As suggested by Guruprasad Gorthala , you can even try to initially reduce the GO by chemical method and further reduction can be by annealing it. if you control the coating volume ,area and the reduction temp, you can somewhat achieve similar conductivity.