During the decomposition of C 1s XPS spectrum, the sp2 peak (284.7 eV) of the sample contains high a mount of diamond is shifted to the high binding energy side when comparing to sp2 (284.5 eV) of other samples?
0.2 eV is a pretty small shift as for XPS. Charging may easily result in such binding energy difference,
You can find an answer in our paper and references therein:
https://www.researchgate.net/publication/263591416_Spectroscopy_of_carbon_From_diamond_to_nitride_films
Article Spectroscopy of carbon: From diamond to nitride films
Thanks a lot for your concern and the valuable answers.
It is used my research to characterize the thin film hard coatings.
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