I want to prepare graphene oxide around zeta size 20d.nm. Do you know, how to procedure to make the small size GO? Or any companies make the GO around 20d.nm, please give the company information.
Quantitative investigation of the fragmentation process and defect density evolution of oxo-functionalized graphene due to ultrasonication and milling
https://dx.doi.org/10.1016/j.carbon.2015.10.021
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- Ultrasound, Pulsed mode, external refridgeration -> particles properties do not change, but size gets smaller.
- Ultrasound without refridgeration -> particles begin to decompose, you loose functional groups due to CO/CO2 evolution. but process can be done faster than the method with external refridgeration to