Hi! I am trying to make tensile dog bones of PVA for mechanical testing using compression molding but I am having some issues.

At first, I am just trying to make films using the hot press before moving on to the dogbone mold. I cannot get the PVA to start melting until about 230C. At that point, the PVA yellows quite a bit, likely due to thermal degradation. Additionally, there are still a lot of bubbles in the film that I cannot seem to get out.

What is the best way to make tensile dogbones of PVA for mechanical testing?

Thanks!

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