A little more information would be nice... which type of fibres (glass, synthetic, metallic...) ?
But there are quite a few ways to look at fibres within a cement or polymer matrix : cut up a small piece and produce embedded metallographic sections for SEM imaging, X-Ray volume tomography (phase contrast, I think), for instance
The homogeneity of fiber dispersion in a cement matrix is crucial in determining the effectiveness and performance of fiber-reinforced concrete (FRC). Confirming that the fibers are evenly distributed within the matrix ensures the desired properties and behavior of the composite material. The most common technique used to verify the homogeneity of fiber dispersion is the visual inspection of the hardened concrete. This method involves visually examining the surface of the concrete for any signs of segregation or clustering of fibers. It is a qualitative and non-destructive method of assessing the distribution of fibers in the matrix.
However, this method does not provide quantitative data and may need to be more accurate to detect slight variations in fiber dispersion. Another approach to confirm the homogeneity of fiber dispersion is using image analysis techniques. This method involves taking microscopic images of a thin section of the concrete and using digital image analysis software to measure the distribution of fibers. The software can analyze the photos and provide fiber length, orientation, and spacing data. It can also highlight any areas of uneven fiber dispersion, allowing for a more accurate assessment of the homogeneity. However, this method is time-consuming, and the results may vary depending on the image analysis software used.
In recent years, non-destructive testing (NDT) techniques have gained popularity in assessing the quality of concrete. NDT methods such as ultrasonic pulse velocity (UPV) and impact-echo (IE) have been used to determine the distribution of fibers in a cement matrix. These techniques rely on measuring wave velocities and reflections to detect any changes in the concrete's properties due to the presence of fibers. Studies have shown that NDT techniques can provide accurate and quantitative data on the homogeneity of fiber dispersion (Ahmad et al., 2021). However, these methods require specialized equipment and trained personnel, making them more suitable for laboratory testing than on-site inspections. Apart from these methods, destructive techniques can also be used to confirm the homogeneity of fiber dispersion. These methods involve extracting core samples from the concrete and analyzing them using scanning electron microscopy (SEM) and energy-dispersive X-ray spectroscopy (EDX). These techniques can provide high-resolution images of the concrete's internal structure, allowing for a detailed assessment of the fiber dispersion.
However, these methods are time-consuming, costly, and destructive, making them more suitable for research than routine quality control in the construction industry. Furthermore, to these techniques, several studies have proposed using computer-aided methods to confirm the homogeneity of fiber dispersion (Yu et al., 2019). These methods involve creating three-dimensional (3D) digital models of the concrete incorporating the fibers' characteristics and simulating their distribution. Computer simulations can provide valuable insights into the behavior of fiber-reinforced concrete, and they have shown promising results in confirming the homogeneity of fiber dispersion. However, these methods require specialized software and expertise, and their accuracy still needs to be improved compared to physical testing methods.
Various methods and techniques are available to confirm the homogeneity of fiber dispersion in a cement matrix. Visual inspection, image analysis, NDT techniques, destructive testing, and computer-aided methods have advantages and limitations. Therefore, combining these methods and carefully evaluating their results are necessary to accurately assess the fiber dispersion in a concrete composite. Standardization and guidelines for testing and quality control of fiber-reinforced concrete can also ensure more consistent and reliable results. Further research and advancements in testing procedures will help develop more efficient and accurate methods to confirm the homogeneity of fiber dispersion in FRC.
References:
Ahmad, Z. A., Bhat, N. M., Hakeem, A. N., & Baba, A. A. (2021). Non-destructive evaluation of fiber dispersion in cement composites using ultrasonic pulse velocity: Construction and Building Materials, 271, 121542.
Yu, Y., Wei, X., Jin, W., Wang, G., & Fan, Y. (2019). Three-dimensional discrete element method analysis of fiber orientation and distribution in a concrete material. Construction and Building Materials, 205, 330-337.