Comparison between the FTIR spectra between reactants and products should be enough to confirm the qd formation. However, you can try other techniques such as 13c-cp-mas nmr or
Depending on how the qds are (for example, if they are in suspension), you could use electron microscopy (HRSEM/HRTEM). If the qd are confined within a structure (for example, a microporous material such as a zeolite), XPS (depth profiling) could be used to identify how the carbon level increases as the sputtering of the sample progresses.