When I introduced Iron based materials under calcination. I could not control the oxidation state of Iron form Fe2+ to Fe3+. If there is any way to control the oxidation state.
What is the role of inert gas when the materials is under calcination?
when we introduced a material in calcination at high temperature in inert atmosphere. Due to thermal energy, lower energy element that combined with the prepared materials like nitrogen, oxygen, carbon etc. These materials gets thermal energy and emerge out from the prepared sample in gaseous form. So what is happen ? when the material is subjected to inert atmosphere.