How can I extract MCPD in oil and determination with GC-MS?

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How can I extract MCPD in oil and determination with GC-MS?

Hello everybody I am going to extract MCPD in oil ,but I havent pressurized liquid extraction. How can I extract MCPD in oil and determination with GC-MS?

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Isam Eldin Hussein Elgailani

Please look at the following below links which may help you in your analysis:

https://www.gerstel.com/pdf/AppNote-191.pdf

https://ec.europa.eu/jrc/sites/jrcsh/files/eur_24356_en_3-mpcd_esters_in_edible_oil.pdf

Thanks

Safia Taleb

Hi,

May be, if you could identify MCPD, that's better!

So that all of us knew what this compound is?

Mark Krause

It's quite volatile. Headspace should work quite well.