I don't mean low scan rate and high scan rate capacitance value being low or high. I want to ask these types of questions? How are the reactions affected by the scanning rate for 1000 cycles in cyclic voltammetry? Why is only 50 mV/s speed used for 1000 cycles? but for 5 cycles, for example, 2, 5, 10,30, and 50 mV/s speeds are used?
the choice of experimental conditions depends on the aim and on the kind of material you are interested. There is not a recipe valid for all the cases, but a procedure that could be similar for different materials
Dear all, scan rate (and time) should be adjusted to achieve and preserve electron transfer without loss (by side chemical reactions for example when time is allowed). The question was the subject of many RG thread discussions. Please check the links below. My Regards
https://www.researchgate.net/post/How_to_choose_the_right_scan_rate_for_cyclic_voltammetry
https://www.researchgate.net/post/How_does_peak_change_with_scan_rate_in_cyclic_voltammetry
https://doi.org/10.1080/10667857.2015.1133157
https://www.ceb.cam.ac.uk/research/groups/rg-eme/Edu/linear-sweep-and-cyclic-voltametry-the-principles
https://chem.libretexts.org/Bookshelves/Analytical_Chemistry/Supplemental_Modules_(Analytical_Chemistry)/Analytical_Sciences_Digital_Library/JASDL/Courseware/Analytical_Electrochemistry%3A_The_Basic_Concepts/04_Voltammetric_Methods/A._Basics_of_Voltammetry/02_Potential_Sweep_Methods/b)_Cyclic_Voltammetry/ii)_Important_parameters_in_CV
https://chem.libretexts.org/Courses/University_of_California_Davis/CHE_115%3A_Instrumental_Analysis_-_Lab_Manual/Lab_1%3A_Cyclic_Voltammetry
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