Equilibrium melting point and DSC?

02 February 2017 1 5K Report

Can any one tells me how to practically design method on the DSC instruments for Equilibrium melting point determination of a polymer---please step by step

Florian J. Stadler

This is not my special area, but if I am not completely wrong, you need to do the following things:

1. run heating scans by DSC at different heating rates.

2. plot melting points vs. heating rate and extrapolate for q=0 K/min

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