01 April 2019 3 7K Report

Taking AgPF6 from the glovebox I see an 19F NMR signal that is not PF6 that is ~0.8% present. Upon leaving the AgPF6 exposed to atmosphere the intensity of the 19F NMR signal increases. I have search everywhere and cannot find any literature on what the impurity is? Any help would be much appreciated.

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