Can anyone share any experiance relating to synthesizing pyrazole from chalcone through sonochemical method?
My chalcone were synthesized from 4-hydroxyacetophenone and DMAB
I have tried to react my chalcone with HCl followed by hydrazine hydrate 80% under ultrasonic irradiation for 4 hrs.
but the result is not satisfying as the chalcone was not completely reacted (remains).
any suggestion