I start to fabricate Lead halid perovskite thin films, and I am trying to get HPbI3 film first as the intermediate material. But I don't know how to prepare this material using my esisting vacuum equipments. Thank you very much!
HPbI3 powders were prepared by mixing PbI2 and hydroiodic acid in DMF with stirring for 1 h. The obtained residue of HI is washed by diethyl ether. The final product are stored in an oven at 40 to 45 °C. I hope the following articles will help you to make solution based HPbI3 powders,