We pretend to use 3-4-dymethylpyrrole as a monomer for conducting polymer. Nevertheless, we haven´t found any reference, concerning its synthesis and(or) polymerization. Do you have any suggestions concerning its synthesis?
many paper could be referred:
(1) Synthesis and michael reaction of 3, 4-dimethylpyrrole. Journal of Heterocyclic Chemistry, 1976, 13(5): 1145-114
(2) Syntheses of 3, 4-Dimethylpyrrole. Bulletin of the Chemical Society of Japan, 1976, 49(4): 1157-1158
(3) Intercalative polymerization of 3-methyl-and 3, 4-dimethylpyrrole in the VOPO4 interlayer space. Chemistry letters, 1993, 22(1): 31-34
Volodymyr
Here is some more references
---Byun, Young Seok and Lightner, David A. Journal of Organic Chemistry, 56(21), 6027-33; 1991
---Baldwin, Jack E. and Bottaro, Jeffrey C. Journal of the Chemical Society, Chemical Communications, (11), 624-5; 1982
---Roth, Steven D. et al Tetrahedron, 63(45), 11030-11039; 2007
---Kancharla, Papireddy and Reynolds, Kevin A. Tetrahedron, 69(39), 8375-8385; 2013
---Robben, Uwe et al Journal of the American Chemical Society, 130(34), 11303-11311; 2008
---Chen, Qingqi et al Synthetic Communications, 32(7), 1031-1040; 2002
Good luck
You can buy it - richman chemical : http://www.richmanchemical.com/
Stuff has a unique smell.... used it on a project I did way back when - but previous workers had left me a more than sufficient stash, so I never had to make it. Keep it frozen. Because it was not a new compound, the prep isn't in any publications we put out, but is in my colleagues dissertation: Alvin D. Joran, California Institute of Technology, 1986, "Photochemical Electron Transfer at a Fixed Distance" - he was very meticulous in recording his preps, I have often gone back to his dissertation for reproducible syntheses.
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