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I am using the MRM to quantify the heparin disaccharides, based on the papers the LOQ is around 10 pg, but I just can get the around 300 pg? And the training engineer didn't give good suggestions....
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So far I am trying the LC-MSMS MRM to quantify my sample, before the training engineer comes, I can do the LOQ is 300 pg, the training engineer changed the spray needle, ion transfer tube and the...
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