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In my experience doing cyclic voltammetry glassy carbon (GC) can be used up to 1.8-2.0 V vs. Ag/AgCl in MeCN water mixtures, without visible degradation of the electrodes. For graphite electrodes...
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Does anyone know of a paper where the formal oxidation potential of H2O to O2 in non-aqueous solvents, specially propylene carbonate and acetonitrile, has been measured or estimated?
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Also If anyone has done it and has some advice, they would be welcome! Thank you
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I have a discrepancy with some published spectra but NMR data indicates we've obtained it almost pure
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