Trying to synthesize malonyl dichloride from malonic acid using POCl3 but no reaction is observed. What to do to help the reaction take place?

I'm trying to synthesize malonyl dichloride from malonic acid using POCl3 as the chlorinating agent. I'm adding dropwise the POCl3 at 0 Celsius degrees to the solid malonic acid and stirring the...

08 February 2023 7,408 1 View