Brent Banasik

2 Questions 4 Answers 0 Followers

Questions related from Brent Banasik

Is there a good protocol for preparation and purification of phosphoryl chloride (POCl3)?

I am looking to synthesize POCl3 from PCl5 and B(OH)3. I believe this to be an industrially used process, but I cannot find any recipes for preparation. Any help would be very much appreciated!...

18 October 2016 4,154 7 View

Could sodium sulfate surfactants be reacting/decomposing with DMSO?

I have synthesized a sodium sulfate surfactant. The starting material is soluble in CDCl3 and has a nice NMR spectrum. When i try to NMR my product in CDCl3 there was zero analyte (this is...

12 October 2016 9,903 4 View