What is the exact conditions, such as temperature, solvents, catalysts, reagents, and procedure for the preparation of benzothiadiazole from OPD ?

I am trying to prepare benzothiadiazole from OPD and thionyl chloride in presence of triethyl amine (solvent; Toluene). the reaction was monitored with the help of tlc, a very weak fluorescent...

28 June 2024 6,762 0 View