Alexandra Dillon

2 Questions 2 Answers 0 Followers

Questions related from Alexandra Dillon

What are reaction conditions for aromatic sulfonation of a dibenzyl ether derivative?

I am using chlorosulfonic acid in chloroform (inert, 2 hr, RT) to para-sulfonate benzyl groups on a dibenzyl ether. The work up is extraction with water. The reaction, however, does not seem to...

05 August 2020 4,564 7 View

Steglich Esterification with EDC/DMAP in CH2Cl2 Extraction - How do I remove excess EDC/DMAP?

I am running a Steglich Esterification with EDC/DMAP in CH2Cl2 on a with the carboxylic acid being a potassium salt that is p-sulfonated. Will the sulfonate group be effected by this reaction? I...

26 February 2020 4,959 3 View