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Every method I have tried resulted in a very low yield (5%). In method one, potassium carbonate and amine salt were dissolved in water, followed by the addition of DCM, and stirring for 15 mins...
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I was thinking about scrapping of the silicate layer from TLC plate and using it on another glass plate. From what I read online, this does not sound like it will work, so my question is why not....
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