My sample is an LFP precursor wherein calcination requires inert / nitrogen gas to form LFP. The problem is, in Indonesia I have not found a place to test DSC TGA with nitrogen / inert gas flow. Maybe someone has a network to be able to test in detail, whether in Indonesia or outside Indonesia? Thank you very much
additionally to the above comment, if you have access to a TGA set-up working with air, you just need to replace the air supply by a compressed N2 bottle (or a connection to a N2 line).
Thank you to Thomas Breuer
and Juliette Blanchard for the answer.For the tools at ITB, I have checked, he has a temperature limitation that is a maximum of 500 for dsc tg. Whereas my sample requires at least 800, so it looks like I have to look for a tool elsewhere.
To modify the tool, it might be tried. But if the lab prohibits modifying the tool, it may have to look for other options.
However, thank you for answering my question
It may even not be a modification. Some (most ?) TGA have two gas inputs. You would just need to connect to the second gas input (compressed N2 + appropriate gas regulator)
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