Basically , we notice a lot of offset once the piezo scan is done after the nanoindentation test. This offset is more clearly observed in the forward and reverse scan. Please provide possible reasons for this.
During the nanoindentation process, a calibrated indenter tip approaches the surface of the sample. The force-displacement data is used to determine the point of contact. After the sample is contacted, the force is linearly increased and the tip indents into the surface of the sample.The application of hardness testing enables you to evaluate a material's properties, such as strength, ductility and wear resistance, and so helps you determine whether a material or material treatment is suitable for the purpose you require.The unit of hardness given by the test is known as the Vickers Pyramid Number (HV) or Diamond Pyramid Hardness (DPH). The hardness number can be converted into units of pascals, but should not be confused with pressure, which uses the same units.
Hardness is a characteristic of a material, not a fundamental physical property. It is defined as the resistance to indentation, and it is determined by measuring the permanent depth of the indentation. ... The Rockwell test is generally easier to perform, and more accurate than other types of hardness testing methods.