I am working on sulfide-based solid electrolytes. Due to the high sensitivity of precursors to air and moisture, all the synthesis step has to be done in an argon atmosphere. My question is, whether ball milling followed by pelletisation of the sample ( after heat treatment) should also be carried out in an argon atmosphere?.
Abu Faizal
You have synthesized solid electrolytes in the presence of argon. Dispersion in a mill followed by granulation is a continuation of the chemical process. Small particles of the substance are more active in the reaction than normal particles, so you need to continue grinding and granulating in argon.
Yes. All your stage most be done in argon condition. Becauos your reaction can carry moisture
Because your substance is sensitive, all reaction related to these material must be done at inert atmosphere for getting high percent of reaction
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