After all fine calculations done I am getting XRD pattern which shows that Ca in my reactant is less.
This is an old problem. At room temperature, the decomposition occurs too fast. Hence, the crystals must be kept below 0C. See the attached paper for more insights.
If we have a new sample and we do not know its space group than how we can determine or confirm its xrd pattern (2theta vs intensity) .
02 March 2014 2,368 12 View
Can we get impurity phases due to chemical that is 99.9 percent pure since they are not 100 percent pure?
31 December 2013 5,393 2 View
My compound shows some extra phases other than the product, so it is due to the amount of Ca or Ba in their carbonates.
11 December 2013 5,896 6 View
I just want to know whether we can get good XRD data in less time by making our slide better. One way to get good data is to make the powder as fine and uniform as possible. What other parameters...
11 December 2013 9,949 5 View
Like if I need to make ABCO3, here A, B, C are any metal and O is oxygen, now if i fulfil the charge constrain, now on what basis i will have the surety whether the compound will be formed or not?
10 November 2013 7,291 5 View
effect of double bond on the flexibility of polymers
07 April 2021 0 0 View
I am writing to request some information for making polymer color flakes. I would appreciate the help.
17 March 2021 0 0 View
In physics, the description of the properties of light generally refers to its wavelength (nm), while in the range of microwaves and radio waves we refer to the frequency of a signal (e.g. kHz or...
03 March 2021 1,682 3 View
03 March 2021 8,272 1 View
I have dataset which shows the length of power lines. I need to classify the lines based on the line length. Is there a rule to classify the High voltage (HV) and low voltage (LV) lines based on...
03 March 2021 4,116 4 View
I looking for ferro calcium production process
03 March 2021 1,755 4 View
Hello, I have a mechanism where air rises due to convective flows. In this simulation, nothing is driving the air except this. I understand that the Boussinesq approximation only works for small...
02 March 2021 4,910 3 View
Hello everyone. Given microstructure image belongs to a 12% ledeburitic cold work tool steel (annealed and tempered). The sample was etched with picral (100 mL ethanol and 4 g picric acid). I...
02 March 2021 4,119 3 View
Hello, I am working on the photocatalytic degradation of PEG 400. I would like to know if it's possible to determine the degree on polymerization based on NMR integration, or by the MW of the...
02 March 2021 6,186 3 View
(This statement is from wikipedia, BTW). What is so special about metallic bond that is limiting high-P low-T state of a matter (as long as individual atoms exist, not white dwarf of neutron star...
02 March 2021 3,309 2 View