I am currently performing some cyclic voltammetry on a MoSe2 semiconductor. I get some noise in the photocurrent region that I cannot explain. I've already seen this effect on voltammograms with TiO2 under illumination. Does anybody know about this?
What kind of light source do you use? Probably the noise originates from poor stability of light source or/and external sources (like room lamps, windows, etc.).