I'm supposing you are dealing with a polycondensation syhthesis. There is a lot of information regarding REX, please look for it carefully.

I'm supposing you are dealing with a polycondensation syhthesis. There is a lot of information regarding REX, please look for it carefully.

You are dealing with reactive extrusion, that you can not rediscover as it is known for long. You need a special extruder for this, allowing outgassing of volatile producrs indeed. Neither you can rediscover this technique nor it can be summarised here within a few lines. There is a lot to learn from your library.

Alain

Thanks for the information. Will look around and hope to find my answers :)

Maybe you can have a look at the following PhD Thesis:

Titel: Reaktive Extrusion von Polyamid 6/Polyether-Blockcopolymeren und deren Einsatz als Schlagzähmodifikatoren in Polyamid 6

Band 1 von Schriftenreihe, Universität Stuttgart Institut für Kunststofftechnik

Verlag Inst. für Kunststofftechnik, 2014

Länge 119 Seiten

written at "Institut für Kunststofftechnik" - University of Stuttgart

unfortunately it is written in german, but there is an english abstract.

Stefan

Dear Ankur, I agree with previous answers. I want to focus that the starting viscosity of your reagents is much important for having success in this sythesis. I do not know what kind of monomers you will use, but keep into accont the possibility of preparing pre-polymers. Regards