Hello!
Does anyone have a hand on experience of 3,7-dibromophenothiazine preparation/synthesis? I have tried many protocols including Br2 in AcOH and NBS in DCM or THF. All in vain. Pour in your experience please. Thanks
I am new to research. The boiling point of triethyl amine (NEt3) is 89 degrees centigrade. I am skeptical that when I will let the hydrogen escape which is getting generated in situ, I will also...
21 July 2024 7,284 4 View
i want to delete my research paper.
09 July 2024 6,554 2 View
I'm working on the proteome (from Uniprot), as you're probably aware that there are reviewed and unreviewed proteins, however unreviewed proteins are in large quantities, but reviewed proteins are...
09 July 2024 5,782 2 View
I am trying to run LDH assay on my samples using Hroiba ABX pentra 400. Multical has worked but negative and pos control are showing an error message saying no control in memory (image attached)....
18 June 2024 6,514 0 View
I have nearly completed my preparation for the short communication. However, I could use some assistance with the results. Any help would be greatly appreciated.
12 June 2024 4,230 1 View
How to calculate sample size for Quasi-Experimental Design Research?
21 May 2024 9,555 3 View
suggest research regarding this topic
17 May 2024 9,366 0 View
Some people suggest that the introductory chapter of the dissertation should consist of subheadings compared to the literature review chapter? Can anyone please confirm which is more acceptable?
15 May 2024 4,037 1 View
What is the difference between conceptual framework and working model while writing the dissertation?
12 May 2024 6,306 1 View
Perform Experiment and report
11 May 2024 3,449 1 View
I perform al alkylation reaction on an imdazole compound where the alkyl reagent (1-Iodo-Octane) was in excess. After the reaction was completed, I then performed an extraction, followed by...
24 May 2024 8,042 2 View
I'm trying to synthesize a highly polar compound which is uv inactive (In TLC charring at the bottom- 0.1RF/20%MeOH:DCM ,MP) . I have confirmed the compound by simple mass and H'NMR spectrums but...
22 May 2024 9,818 3 View
Practically it forms gel
10 March 2024 3,127 1 View
I mixed 20 ml water with 10 ml DCM in funnel. I separated the organic phase and I analysed it with GCMS. The concentration is too low.
14 February 2024 7,697 5 View
I tried DMF( 100%), and DCM:DMF, in different rations, for DCM:DMF(4:1) I found elastin fiber mate with so many beads.
24 January 2024 9,245 3 View
Shouldn't the difference in intensity of the compound be higher when DCM is used as a solvent than methanol in GC-MS analysis? I will analyze phthalates and organic phosphorus flame retardants...
07 December 2023 8,556 2 View
4-(2-Thiophenestyryl)-1-methylpyridinium iodide (compound A) is attach on both side of my compound. first i thought it is polar molecule but it has not high polarity. I did column chromatography...
03 November 2023 1,522 0 View
i'I'mm interested in extracting phenolic resin using a microwave (MAE) method from Gracinia sp., but there are very few reviews available. So, I asked someone who knew. Why does it give good...
14 October 2023 3,290 3 View
Does anyone know where I could purchase gold-core silver-shell nanoparticles in a dichloromethane solvent? Our usual supplier only seems to have them in water.
02 October 2023 9,483 2 View
Dear all, I am currently working with a GC-MS/MS system, and I've used HPLC-grade solvents in my experiments. Recently, I came across the availability of GC-MS-grade Dichloromethane (DCM). I'm...
14 September 2023 8,706 2 View