I didn't get Raman Spectra of carbonaceous phase from a composition of Mg/C based condensed powder obtained by arc-plasma method. However, Raman spectra is observed when the powder sample has been processed by severe plastic deformation techniques under very high pressures and at room temperature. My question is why there are no spectra from carbon materials at the powder state ? What could be the possible nature of carbon phase in the powder materials after arc-plasma processing ? I know very little about the Raman Spectroscopy for carbonaceous materials. If someone is expertise in this field, please help me to find out the root cause for this interesting phenomenon.