I want to know about the chemical synthesis procedure of Chromium (III) Iodide (CrI3). If you find any method for synthesis of Chromium (III) Iodide (CrI3) in soft chemical route then kindly let me know.
Chapter Chromium (III) Iodide
Thank you Prof. Merola.
direct reaction of chromium metal with an excess of iodine. The reaction is conducted at 500 °C:
2 Cr + 3 I2 → 2 CrI3
To obtain high purity samples, the product is thermally decomposed at 700 °C to sublime out chromium(II) iodide. The diiodide is then renominated.
Gregory, N. W., Handy, L. L. "Chromium(III) iodide" Inorg. Synth. 1957, vol. 5, 128-130.
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