Bromination of 2-nitro toluene in EDC with Bromine & AIBN, hydrolysis with Na2CO3 gave two high boiling impurities. Guess the Impurities please?

13 August 2020 0 5K Report

Actually I tried bromination of 2-nitro toluene with Br2/AIBN in presence of EDC/H2O and the hydrolysed with Sodium carbonate gave alcohol. But I got two impurities at high boiling point in GC and also those impurities not detected in HPLC. Can any one help me to find that impurity structure?

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