Dear beloved fellow chemists,
I am having trouble derivatizing Inorganic Bromide by Propylene Oxide (H2SO4 catalyzed reaction). I seem to get almost no product by the EURL-SRM method. It's an Electron Capture Detector method that I'm trying to run by GC/MS/MS. I do see the ISTD no problem though.
In addition, any hang-ups on derivatizing Dithiocarbamates to CS2 by the "Automated Headspace GC in Plant matrices" method? Thank you all.-Paul D. Dodson
Hi Paul,
do you know this article?
Article Validation of single residue methods for the determination o...
Regards
Markus
Markus,
Thank you so much for this article. I have scoured the internet for any references to both of these methods. This definitely elucidates my derivatization problem. VERY MUCH APPRECIATED!-Paul D. Dodson
Thank you, Marcus. Next time we'll have to make sure Paul gives you the shout-out in the title instead of me! Good luck, Paul. It is definitely not easy.
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