How to remove the instrumental broadening when sample synchrotron diffraction peaks are equally or even less broadened than CeO2 or LaB6 powder peaks?

I'm performing modified Williamson-Hall and Warren-Averbach analysis based on data from in situ synchrotron high-energy X-ray diffraction experiments. The materials include mainly various annealed...

23 January 2024 6,203 5 View