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I trying a reaction to protect 5'-OH of a modified nucleoside with DMT-Cl and DIPEA in pyridine. I have used 2 eq of DMT-Cl for 24 hour at room temperature. But the reaction is still incomplete. I...
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I have tried 10% H2SO4 in ethanol (by volume) and then heating at 100ºC for 30 minutes. But It did not work for me. Does anyone have other ideas?
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