How to derivatize Amino Acids using N-tert-butyldimethylsilyl- N-methyltrifluoroacetamide (MTBSTFA) for GC-MS analysis?

I recently attempted to replicate the amino acid derivatization procedure outlined by Sobolevsky et al. 2003. While I followed the steps diligently, unfortunately, I did not achieve the expected...

29 February 2024 7,068 6 View