Any suggestions for a work up for 2-Amino-1-(4-nitrophenyl)-1,3-propanediol after deamidation from chloramphenicol?

I have prepared 2-Amino-1-(4-nitrophenyl)-1,3-propanediol by acid catalysed deamidation of chloramphenicol and confirmed the structure by LC-MS. I need to purify the product and determine its...

30 January 2014 2,540 2 View