Does anyone have Unstable PEDOT film deposited from acetonitrile/LiClO4 solution via electropolymerization on gold electrode?

I am trying to deposit PEDOT film on microfabricated gold electrode. I am using 0.1 M LiClO4, 0.01 M EDOT in acetontrile. Scan rate is 5 mV/s and 50mV/s. Film forming after deposition is not...

12 February 2016 6,873 3 View