How can I purify HCl salt of a compound which has an isocyanate group?

Prashant Gudeangadi @Prashant_Gudeangadi

11 November 2013 1 1K Report

The ring also has 2 nitrogen atoms.

HI Prashant,

It all depends on the nature of the mixture from wich you want to extract your compound. So what are the mates in this mix?

Anyway generally speaking I would try and follow one of the strategies below or a combination

1) cristallisation

2) trituration

3) working with the solubility at different pH (being an hydrochloride salt I assume it has a certain stability in acidic environment which I take is mantained to neutral pH given the absence of efficient nucleophiles)

3) acidic resins (catch and release)

Hope that can help, good luck

Giuseppe

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